|
Тема |
Re: freebasing DPT [re: Gligi] |
|
Автор |
purist (тъпист) |
|
Публикувано | 11.05.04 00:38 |
|
|
през носа понаболяват, но то всичко понаболява (освен ако не се смеси с нещо обезболяващо де ;)). Проблемът е че държи прекалено много време което в конкретния случай с ДПТ е равносилно на психо-тероризъм. Чистото в-во е по-интензивно но и пуска по-бързо.
копи-пасте от еровид за процедурата:
Conversion of Hcl salt to freebase:
2g of DPT Hcl was dissolved in 150ml of water. It was difficult to get the crystals to go into solution and it required a small amount of heat. Be careful not to apply too much heat, as DPT is very heat sensitive. Once the DPT was in solution the water mixture was added to a separatory funnel and ammonia hydroxide was then added dropwise to basify. After each drop I swirled the mixture to distribute the ammonia evenly, observing a white cloud of freebase forming out of solution. When it reached a ph 8-9, I added 75ml of chloroform. This mixture was swirled and thoroughly shaken for about 5-10 minutes with the chloroform layer settling on the bottom. The chloroform extraction was then poured off and saved in a flask. This process was repeated 3 more times, with each extraction requiring additional ammonia hydroxide to keep the ph level at 8-9. The last extraction was left to sit for 5 hours just to make sure that all of the DPT was recovered from the water solution. The combined chloroform extractions were then evaporated in a baking dish leaving a semi-clear-white DPT freebase oil behind. 2g of finely ground dried parsley was added to the baking dish and scraped and thoroughly mixed with a razor blade until the parsley was completely saturated. The mixture was still somewhat sticky but relatively easy to handle. It was then placed in a glass vial for easy use and storage.
"The more you debug it, the more it bugs" - аз
|
| |
|
|
|