|
Тема |
Re: methamphetamine [re: Изyмeн] |
|
Автор | Necron (Нерегистриран) | |
Публикувано | 25.02.06 21:52 |
|
|
Щом 50мг ефедрин струват 1 лев, не си струва изобщо. Само ефедрина ще струва над 30 лева за синтезата на 1 грам метамфетамин, а освен това трябва да се купуват други реактиви, а като прибавиш и труда... Ето все пак най-простата рецепта. Извличането на червен фосфор от кибрити е лесно и няма смисъл да слагам рецептата.
Извличане на йод от йодна тинктура:
Materials:
5% Tincture: 5% I2, 5% KI, IPA, H2O
97% H2SO4 or whatever you have
Bleach (unscented)
Gravity filtration, a buttload of coffe filters
2L pyrex or glass bowl
500 ml mason jar
Procedure:
4 X 25ml (100ml total) of 5% tincture was added to the mason jar. 100 ml of dH2O was added to the tincture. If your anal like I am you can use this water to wash out the remaining tincture in the bottles.
To the tincture/H2O mix there was added SLOWLY 5 ml of 97% H2SO4 with stirring. If you dont have 97 just convert the volume added based on the percentage you do have. Fumes were emitted and the solution heated slightly. Let cool back to room temp. The acid functions to convert KI into HI facilitating the oxidation of iodide to iodine.
Fill the 2L pyrex or glass bowl with 1L of dH2O, set aside.
Add slowly and with good stirring 12 ml of bleach to the tincture/dH2O. Use your good observation skills at this point. You are waiting to see a colour change of the solution from a deep red to a even more deep red/black colour and for the emergence of I2 precipitate. When I2 precipitates, some of it rises to the surface and gives a noticeable "metallic" appearance to the surface.
Add another 12 ml of bleach like you did before all the while, looking for signs of precipitation. ONce you see those signs, IMMEDIATELY (oh, the drama) dump the tincture/dH2O/I2 into that 1L of dH2O you set aside.
Sit back and watch the I2 completely fall out of solution. Let it sit for 20 min. Feel free examine it an ponder about the wonders of the world.
Set up gravity filtration with 2 coffee filters. Filter out the I2. Rinse the bowl with dH2O, add rinse to I2 in filter. Rinse I2 with 500 ml dH2O. This gets rid of any salts. Try to coax the I2 to the center of the filter.
Time to dry out the I2. Put some gloves on (if you haven't already) and gather the edges of the filter and twist them down to wring out the moisture. Keep adding fresh filters on the outside and keep wringing until no more moisture surfaces to the new filters.
Take that wad and squish the hell out of it on a hard surface. Unwrap the wad and transfer I2 to a container. Dessicate under vaccumm. Or just put the container in a bigger one with drying agent and seal shut. Store out of light.
Seelight got 8.2 g of I2 out of 100 ml of 5% tincture. From what info has been gathered on de HIVE, this seem suitable for I2/RP of pseudo.
Редукция на ефедрин с червен фосфор и йодоводородна киселина:
In a 500 mls round-bottom flask is added 150 mls of glacial acetic acid, 15 grams of red phosphorus, and 33.50 grams of iodine.[NOTE 6] The mixture is allowed to react for 15 - 20 minutes, until all of the iodine has reacted. Then add 10 mls of distilled water and mix, then add 8.07 grams (0.04 mole) of EPHEDRINE HCl, and mix. A reflux condenser is added to the 500 mls round-bottom flask and the mixture is gently refluxed (gently boiled continuously) for 2 and 1/2 hours. The hot mixture is suction filtered while still hot to remove the excess red phosphorus. The hot filtrate is added slowly by pouring into a solution of 20 grams of sodium bisulphite in 1 liter of distilled water. The solution is made basic and solvent extracted as above using two 100 ml portions of ether, washed and dry. The oily residue extracted (after removing the ether) is a mixture of methamphetamine, iodo-ephedrine and minor amount of acetic ester ephedrine.
P.S: Moonclub, ти би трябвало да знаеш... какво друго освен червен фосфор, бертолетова сол и лепило има в главите на кибритените клечки?
|
| |
|
|
|